XRD STRUCTURE STUDY ON NICKEL DOPED ZINC OXIDE NANOPARTICLES SYNTHESIZED BY COPRECIPITATION METHOD

Destalina Destalina; Fitriah Mujtahid; Inayatul  Mutmainna; Dahlang  Tahir; Paulus L  Gareso

doi:10.29303/ipr.v5i3.179

XRD STRUCTURE STUDY ON NICKEL DOPED ZINC OXIDE NANOPARTICLES SYNTHESIZED BY COPRECIPITATION METHOD

Authors

Destalina Destalina , Fitriah Mujtahid , Inayatul Mutmainna , Dahlang Tahir , Paulus L Gareso

DOI:

10.29303/ipr.v5i3.179

Published:

2022-08-18

Issue:

Vol. 5 No. 3 (2022)

Keywords:

X-ray Diffraction, Nickel (Ni), A Coprecipitation Method, ZnO nanoparticles

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Destalina, D., Mujtahid, F., Mutmainna, I. ., Tahir, D. ., & Gareso, P. L. . (2022). XRD STRUCTURE STUDY ON NICKEL DOPED ZINC OXIDE NANOPARTICLES SYNTHESIZED BY COPRECIPITATION METHOD. Indonesian Physical Review, 5(3), 188–196. https://doi.org/10.29303/ipr.v5i3.179

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Abstract

Nickel-doped Zinc Oxide (Zn(1-x)Ni(x)O) nanoparticles have been synthesized by the chemical coprecipitation method. The structure and characteristic of synthesized Ni doped ZnO nanoparticles ware analyzed by X-ray diffraction (XRD) patterns. Crystallite sizes and lattice strain of all samples were calculated using the Scherrer’s formula, Uniform Deformation Model (UDM) and Halder-Wagner (H-W) method. X-ray diffraction analysis confirmed hexagonal cubic structure of Ni-doped ZnO nanoparticles. Also, the crystallite size of the nanoparticles reduces as the nickel concentration increase. The result showed the average crystallite size calculated by Scherrer’s formula (25-29 nm) was smaller than crystallite size using UDM method (51-63) the largest average crystallite size and H-W method (42-47 nm). The lattice strain increases with decreasing crystallite sizes value. The crystal size Ni- doped ZnO nanoparticles decreased with increasing dopant concentration.

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XRD STRUCTURE STUDY ON NICKEL DOPED ZINC OXIDE NANOPARTICLES SYNTHESIZED BY COPRECIPITATION METHOD

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