ANALYSIS OF CRYSTALLINE PHASE AND FUNCTIONAL GROUPS OF ZnO FROM PINEAPPLE PEEL EXTRACT
DOI:
10.29303/ipr.v5i3.160Downloads
Abstract
The use of pineapple peel has not been paid attention to because of the lack of public knowledge regarding the content and benefits of pineapple skin. However, it can use pineapple skin for herbal drinks and animal feed. Pineapple peel has phytochemical compounds and bioactive compounds such as ZnO. Therefore, this study was conducted to determine ZnO's crystalline phase and the functional group from pineapple peel extract. Synthesis of ZnO from pineapple peel extract used the green synthesis method, with the following steps: pineapple peel was pounded and stirred by heating at 80°C, and then ultrasonicated. The solution was added with NaOH and centrifuged at 4000 rpm. This result is heated at a temperature of 120°C with a 6 and 12 hours holding time. After that, it cooled to room temperature. The results of XRD analysis obtained the optimal ZnO crystalline phase at a holding time of 12 hours according to the pdf cards database (96-210-7060) and nanocrystalline size of 17.55 nm. The FTIR results on the ZnO sample had an absorption peak of 4000-400cm-1 with functional groups O-H alcohol and phenol, -C=C alkene, C=O, C-O, C-N, and Zn-O. It is hoped to be applied later in the medical and industrial fields by obtaining ZnO samples from pineapple peel extract
Keywords:
ZnO, green synthesis, pineapple peel extractReferences
S. Alfarisa, D. A. Rifai, and P. L. Toruan, “Studi Difraksi Sinar-X Struktur Nano Seng Oksida (ZnO),†Risal. Fis., vol. 2, no. 2, pp. 53–57, 2018, doi: 10.35895/rf.v2i2.114.
M. Sari, Y. Rati, T. M. Linda, Y. Hamzah, and A. S. Rini, “Biosynthesis of ZnO Micro-Nanoflower with Ananas comosus Peel Extract,†J. Aceh Phys. Soc., vol. 10, no. 4, pp. 84–87, 2021, doi: 10.24815/jacps.v10i4.18951.
N. A. Mirgane, V. S. Shivankar, S. B. Kotwal, G. C. Wadhawa, and M. C. Sonawale, “Waste pericarp of ananas comosus in green synthesis zinc oxide nanoparticles and their application in waste water treatment,†Mater. Today Proc., vol. 37, no. Part 2, pp. 886–889, 2020, doi: 10.1016/j.matpr.2020.06.045.
S. Jurablu, M. Farahmandjou, and T. P. Firoozabadi, “Sol-gel synthesis of zinc oxide (ZnO) nanoparticles: Study of structural and optical properties,†J. Sci. Islam. Repub. Iran, vol. 26, no. 3, pp. 281–285, 2015.
N. Seng, O. Zno, D. A. N. Aplikasinya, and S. Agen, “ANTIBAKTERI Staphylococcus aureus INDONESIAN FUNDAMENTAL,†vol. 5, no. 1, pp. 15–25, 2019.
I. S. Saputra, S. Suhartati, Y. Yulizar, and S. Sudirman, “GREEN SYNTHESIS NANOPARTIKEL ZnO MENGGUNAKAN MEDIA EKSTRAK DAUN TIN (Ficus carica Linn),†J. Kim. dan Kemasan, vol. 42, no. 1, p. 1, 2020, doi: 10.24817/jkk.v42i1.5501.
M. M. Chikkanna, S. E. Neelagund, and K. K. Rajashekarappa, “Green synthesis of Zinc oxide nanoparticles (ZnO NPs) and their biological activity,†SN Appl. Sci., vol. 1, no. 1, pp. 1–10, 2019, doi: 10.1007/s42452-018-0095-7.
A. Falih, N. M. Ahmed, and M. Rashid, “Green synthesis of zinc oxide nanoparticles by fresh and dry alhagi plant,†Mater. Today Proc., vol. 49, no. xxxx, pp. 3624–3629, 2020, doi: 10.1016/j.matpr.2021.08.201.
D. Candida, “Jurnal Biology Science & Education 2019 GEMY NASTITI HANDAYANI,†vol. 8, no. 1, pp. 1–8, 2019.
C. N. Aguilar, “SC,†Trends Food Sci. Technol., 2019, doi: 10.1016/j.tifs.2019.01.018.
P. C. Nagajyothi, S. J. Cha, I. J. Yang, T. V. M. Sreekanth, K. J. Kim, and H. M. Shin, “Antioxidant and Anti-inflammatory activities of zinc oxide nanoparticles synthesized using Polygala tenuifolia root extract,†J. Photochem. Photobiol. B Biol., 2015, doi: 10.1016/j.jphotobiol.2015.02.008.
S. Jafarirad, M. Mehrabi, B. Divband, and M. Kosari-nasab, “Biofabrication of zinc oxide nanoparticles using fruit extract of Rosa canina and their toxic potential against bacteria : A mechanistic approach,†Mater. Sci. Eng. C, vol. 59, pp. 296–302, 2016, doi: 10.1016/j.msec.2015.09.089.
S. K. Katiyar, R. Agarwal, and H. Mukhtar, “Inhibition of Tumor Promotion in SENCAR Mouse Skin by Ethanol Extract of Zingiber officinale Rhizome1,†no. 216, pp. 1023–1030.
M. Aminuzzaman, L. P. Ying, W. S. Goh, and A. Watanabe, “Green synthesis of zinc oxide nanoparticles using aqueous extract of Garcinia mangostana fruit pericarp and their photocatalytic activity,†Bull. Mater. Sci., vol. 41, no. 2, 2018, doi: 10.1007/s12034-018-1568-4.
H. H. Basri, R. A. Talib, R. Sukor, S. H. Othman, and H. Ariffin, “Effect of synthesis temperature on the size of ZnO nanoparticles derived from pineapple peel extract and antibacterial activity of ZnO–starch nanocomposite films,†Nanomaterials, vol. 10, no. 6, 2020, doi: 10.3390/nano10061061.
R. Maurischa, A. Putri, T. Yuanita, and M. Roelianto, “Daya anti bakteri ekstrak kulit nanas ( Ananas comosus ) terhadap pertumbuhan bakteri Enterococcus faecalis Antibacterial potency of pineapple peel extract ( Ananas comosus ) on Enterococcus faecalis growth,†vol. 6, no. 2, pp. 61–65, 2016.
D. B. Bharti and A. V. Bharati, “Synthesis of ZnO nanoparticles using a hydrothermal method and a study its optical activity,†Luminescence, vol. 32, no. 3, pp. 317–320, 2017, doi: 10.1002/bio.3180.
C. Paper, H. Hamrayev, and S. Kamyar, “Biopolymer-Based Green Synthesis of Zinc Oxide ( ZnO ) Nanoparticles Biopolymer-Based Green Synthesis of Zinc Oxide ( ZnO ) Nanoparticles,†no. August, 2021, doi: 10.1088/1757-899X/1051/1/012088.
S. Kurajica and I. K. Munda, “Mechanochemical synthesis of zincite doped with cadmium in various amounts,†pp. 482–490, 2019.
N. Jayarambabu, K. Venkateswara Rao, and Y. Taraka Prabhu, “BENEFICIAL ROLE OF ZINC OXIDE NANOPARTICLES ON GREEN CROP PRODUCTION Phytochemical screening and evaluation of in vitro antioxidant and antimicrobial activities of the indigenous medicinal plant Albizia odoratissima View project,†Researchgate.Net, no. February, 2015, [Online]. Available: https://www.researchgate.net/publication/301541596
License
This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.
Authors who publish with Indonesian Physical Review Journal, agree to the following terms:
- Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution-ShareAlike 4.0 International Licence (CC BY SA-4.0). This license allows authors to use all articles, data sets, graphics, and appendices in data mining applications, search engines, web sites, blogs, and other platforms by providing an appropriate reference. The journal allows the author(s) to hold the copyright without restrictions and will retain publishing rights without restrictions.
- Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgment of its initial publication in Indonesian Physical Review Journal.
- Authors are permitted and encouraged to post their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work (See The Effect of Open Access).
